Abstract: Pure Cs ferrite and mixed Cs-Li ferrite have been synthesized by using solution combustion method. For solution combustion method oxalic dihydrazide has been used as a fuel. Solution combustion method leads to the formation of single-phase ferrite materials. By using this method ferrite materials have been synthesized at lower temperature and in shorter time. The identity of synthesized ferrite materials has been established by using Fourier Transform Infrared Spectroscopy (FTIR). As synthesized ferrite materials have been employed for adsorption of dyes from their aqueous solutions. Ferrite materials have proven to be efficient adsorbents due to their nano-sized particles, reusability and easy removal from the solution owing to their magnetic nature.